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响应面法优化氧化辛烯基琥珀酸甘薯淀粉酯的制备工艺 被引量:2

Process Optimization for Synthesis of Octenyl Succinic Anhydride Modified Oxidized Sweet Potato Starch by Response Surface Analysis
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摘要 以氧化甘薯淀粉(oxidation sweet potato starch,OSPS)为原料,制备氧化辛烯基琥珀酸甘薯淀粉酯(octenylsuccinate anhydride-oxidation sweet potato starch,OSA-OSPS)。运用响应面分析(response surface method analysis,RSA)辛烯基琥珀酸酐(octenyl succinate anhydride,OSA)添加量、pH值、温度和时间对OSA-OSPS取代度(degreeof substitution,DS)的影响,得出最佳制备工艺:酸酐添加量7%、pH8.40、温度40℃,反应时间10h。采用快速黏度分析仪(rapid viscosity analyzer,RVA)分析表明:氧化甘薯淀粉峰值黏度较低,而经过OSA酯化后,峰值黏度又会有一定程度的提高,且随DS的增加呈上升趋势。 Oxidized sweet potato starch was used as the raw material to prepare octenyl succinic anhydride(OSA) modified oxidized sweet potato starch.The effects of OSA amount,pH,temperature and reaction time on degree of substitution(DS) of OSA-modified oxidized sweet potato starch were studied employing response surface analysis.The optimum process conditions determined were as follows: OSA amount 7%,pH 8.40,temperature 40 ℃,and reaction time 10 h.Rapid viscosity analyzer(RVA) analysis showed that the peak viscosity of sweet potato starch decreased after oxidation,and increased after furthermodification with OSA with a positive correlation with DS.
出处 《食品科学》 EI CAS CSCD 北大核心 2011年第20期13-16,共4页 Food Science
基金 四川省科技支撑计划项目(2009NZ0077-007)
关键词 甘薯淀粉 响应面分析 辛烯基琥珀酸酐 sweet potato starch response surface analysis(RSA) octenyl succinate anhydride(OSA)
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