摘要
目的:建立柴辛鼻敏康颗粒的质量标准。方法:采用薄层色谱(TLC)法对方中柴胡、细辛进行定性鉴别;采用高效液相色谱法对芍药苷进行含量测定。结果:TLC斑点清晰、易于识别、重复性好;芍药苷进样量在0.512～15.360μg范围内与峰面积积分值呈良好线性关系(r=0.9998),平均回收率为99.87%,RSD=0.97%(n=6)。结论:该质量控制方法简单、准确度高、专属性强,可有效控制柴辛鼻敏康颗粒的质量。
OBJECTIVE：To establish the quality standards of Chaixin biminkang granules. METHODS：TLC was adopted to identify Bupleuri Radix and Radix Et Rhizoma. HPLC method was used to test the content of paeoniflorin. RESULTS：TLC spots were clear,distinguished and reproducible. The linear range of paeoniflorin was 0.512～15.360 μg（r=0.999 8） with an average recovery of 99.87%（RSD=0.97%,n=6） . CONCLUSION：The method is simple,precise and specific and has good effect on quality control of Chaixin biminkang granules.
出处
《中国药房》
CAS
CSCD
北大核心
2011年第19期1800-1802,共3页
China Pharmacy
