摘要
目的:建立麝香接骨胶囊中松香酸的检查方法。方法:采用Zobarx SB-Aq C18色谱柱(4.6mm×250mm,5μm);流动相:甲醇-0.1%甲酸(80︰20);流量:1mL.min-1;检测波长:241nm。结果:能检查出麝香接骨胶囊中的松香酸。结论:本方法简便、结果准确且专属性强。
Objective: To establish a method for the inspection of abietic acid in Shexiang Jiegu capsule. Methods: The separation was performed on a ZORBAX SB-Aq C18 column (250 mm× 4.6 mm, 5 μm). The mobile phase was consisted of methanol-formic acid (80:20, v/v). The flow rate was 1.0 mL·min^-1. The UV detection was set at 241 nm. Results: The method can inspect abietic acid in Shexiang Jiegu capsule. Conclusion: The proposed method is simple, accurate and exclusive.
出处
《药学与临床研究》
2010年第5期499-500,共2页
Pharmaceutical and Clinical Research