摘要
目的:研究舒胸片6种成分在5种大孔树脂上的吸附-脱吸附性能。方法:分别以相对比吸附量(RA)、洗脱率为指标,考察舒胸片提取液中人参皂苷Rb1等6种成分在HPD-100等5种大孔树脂上的静态吸附和脱吸附性能。并在此基础上比较了综合吸附-脱吸附性能。结果:6种有效成分在5种树脂上的综合吸附-脱吸附性能以人参皂苷Rb1最好,羟基红花黄色素A最差;5种树脂对6种有效成分的综合吸附-脱吸附性能以HPD-100和LSA-30两种树脂相对为佳。结论:实验结果为合理确定舒胸片混合提取液的大孔树脂分离纯化工艺条件提供了实验依据。
Objective:To study the adsorption and desorption properties of macroporous resins to the active components of Shuxiong Tablets. Method:The relative adsorption ratio and desorption rate were used as the evaluating criteria,the static adsorption and desorption capability of 6 active ingredients 5 kinds of macroporous resins such as LSA-7,D101A,HPD-100 were compared. And on this basis,comprehensive properties of adsorption and desorption were compared. Result:Among 6 kinds of ingredients,ginsenoside Rb1 had the best comprehensive properties. And the worst was hydroxy safflower yellow A. A mong the 5 kinds of macroporous resins. HPD-100 and LSA-30 macroporous resins had relatively the optimum comprehensive properties of adsorption and desorption. Conclusion:The experimental results will provide an basis for establishing the feasible purification techrigque of Shuxiong Tablets.
出处
《中国实验方剂学杂志》
CAS
北大核心
2010年第10期5-7,共3页
Chinese Journal of Experimental Traditional Medical Formulae
基金
湖南省教育厅重点课题(07A049)
湖南省科技厅科学研究项目(2008sk3068)
关键词
舒胸片
大孔树脂
静态吸附
脱吸附
相对比吸附量
洗脱率
Shuxiong Tables
macroporous resins
static adsorption
desorption
relative adsorption ratio
desorption rate