摘要
以3,5-羟基苯乙酮为原料,通过乙酰化、还原、甲磺酰化、烯键化4步反应合成了标题化合物,总收率72.7%。通过1HNMR确定了化合物的结构。
3,5-Diacetoxystyrene was prepared through acetylation,hydrogenation,methanesulfonylation and elimination reactions.The overall product yield reached 72.7%,and its structure was confirmed by 1HNMR spectroscopy.
出处
《化学试剂》
CAS
CSCD
北大核心
2010年第7期671-672,共2页
Chemical Reagents
