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双(3-氨基苯基)苯基氧化膦的合成与表征 被引量:3

Synthesis and characterization of bis(3-aminophenyl)phenyl phosphine oxide
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摘要 以三苯基氧化膦为原料,通过硝化和还原反应合成了标题化合物,并采用差示扫描量热法、红外光谱、核磁共振和质谱等方法对产品进行了表征。 Bis(3-aminophenyl)phenyl phosphine oxide(BAPPO)was prepared in this paper via nitration of triphenylphosphine oxide and reduction of bis(3-nitrophenyl)phenyl phosphine oxide,and the product structure was characterized by DSC,FT-IR,1HNMR and MS.
出处 《化学试剂》 CAS CSCD 北大核心 2010年第5期470-472,共3页 Chemical Reagents
关键词 双(3-氨基苯基)苯基氧化膦 双(3-硝基苯基)苯基氧化膦 硝化反应 还原反应 bis(3-aminophenyl)phenyl phosphine oxide bis(3-nitrophenyl)phenyl phosphine oxide nitration reduction
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