摘要
报道了以盐酸三乙胺作催化剂,4,5,6,7位氯代吲哚-3-甲腈和叠氮化钠在DMF中反应生成4个相应的5-(氯代吲哚-3’-基)-1H-四唑类化合物,其结构通过熔点、IR和^1H—NMR等得到确证,纯度〉99.0%。
Four new indolyltetrazole compounds have been synthesized by the addition of sodium azide to 4,5,6, 7 - position ehloroindole - 3 - earbonitriles by the catalyst of triethylarnine hydrochloride. Their structures were confinned by melting point, IR and 1H -NMR.
出处
《化工时刊》
CAS
2010年第4期13-15,共3页
Chemical Industry Times
关键词
取代吲哚-3-甲腈
5-取代四唑
叠氮化钠
substituted indole - 3 - earbonitrile 5 - substitutedindolyl tetrazole NaN3