摘要
目的：建立弱极性毛细管柱顶空气相色谱测定生活饮用水中7种卤代烃的方法。方法：选择弱极性毛细管色谱柱,采用顶空进样方式,确定适宜的仪器分析条件,并对分离度,回收率,精密度及稳定性进行了研究。结果：方法的标准曲线相关系数在0.9985-0.9998之间;相对标准偏差为1.02%-4.77%;回收率为76%-94%。结论：该方法可以快速准确的同时测定水中7种卤代烃。
Objective：To establish a method for determination of halogenated hydrocarbons in drink water by infirm polarity capillary column GC with headspace.Methods：To choose the best determination condition,to decide eligible temperature and flow rate of carrier gas,and study the resolution.Results：The standard curve coefficient correlation was in the range of 0.9985-0.9998.The relative standard deviation was in the range of 1.02%-4.77%.The recovery was in the range of 76%-94%.Conclusion：The method can be used to simultaneous measure 7 halogenated hydrocarbons in water quickly and precisely.
出处
《中国卫生检验杂志》
CAS
2010年第2期289-290,共2页
Chinese Journal of Health Laboratory Technology
关键词
弱极性毛细管柱
顶空气相色谱
生活饮用水
卤代烃
Infirm polarity capillary column
GC with headspace
Drink water
Halogenated hydrocarbons
