摘要
辛醇和顺丁烯二酸酐在酸根的作用下可以生成顺丁烯二酸-2-乙基已酯。采用阳离子交换树脂作催化剂,醇过量的方法制取顺丁烯二酸-2-乙基已酯。考查了反应温度,催化剂用量,酸醇比,反应时间等条件对反应转化率及收率的影响,确定了最佳反应条件,并指出合理的转化率应该在98.2%-98.5%。
Synthesis Diisooctyl Maleate by using maleic anhydride and iso -octanol as materials, ecess mole ratio alcohol to anhydride is used, studied the effect of catalyst, temperature, mole ratio and reaction time on the yield. , got the optimal reaction condition and point out that the reasonable yield should be 98.2% - 98.5%.
出处
《辽宁化工》
CAS
2009年第7期447-448,452,共3页
Liaoning Chemical Industry