摘要
本文讨论了二乙撑三胺五乙酸(DTPA)合成原理和制备方法,研究了反应温度、反应时间、洗水用量、洗涤次数、酸化pH值与酸种类、重结晶溶液浓度等因素对DTPA产率的影响。本研究探索出提高DTPA产率的最佳工艺参数和简单可行的实施方法。主要质量指标(产率大于70%,纯度大于99.
This paper has described the principle of synthesis of diethylenetriamine pentaacetie acid (DTPA)and its preparation process.And investigated the influences of reaction times and quantity of washing water、time、temperature、feeding differ in acid pH value、recrystalligation Concentration on the productivity.DTPA developed has excellent properies,and the technical specification(purity≥99.3% productivity≥70%)has reached the similar advanced product standard in the world.
出处
《山东化工》
CAS
1998年第2期1-4,共4页
Shandong Chemical Industry
基金
山东省教委资助
关键词
二乙撑
三胺五乙酸
氨羧络合剂
络合剂
productivity,diethylenetriaminepentaacetic acid,complexones.