摘要
以二（１，３－二硫杂环戊烯－２－硫酮－４，５－二硫）合锌酸四乙基铵盐（Ｉ）为原料，合成四种未见文献报道的４，５－亚乙二硫基－１，３－二硫杂环戊烯－２－硫酮及酮ＩＶａ，ＩＶｂ，Ｖａ，Ｖｂ，其中由路线Ａ和Ｂ分别制得了Ｖａ；对ＩＶｃ和由路线Ａ制备Ｖｂ失败的原因进行了讨论。
ethylenedithio 1,3 dithiole 2 ones IV a, IV b,V a,V b were prepared from Bis(tetraethylammonium) bis (2 thioxo 1,3 dithiole 4,5 dithiolate)Zincate(I), The compound V a have been prepared through route A and B. Attamput of synthesis of IV c and V b from route A was unsuccessful, The reason for lack of the expected products was discussed.
出处
《西北大学学报（自然科学版）》
CAS
CSCD
北大核心
1998年第1期41-43,共3页
Journal of Northwest University（Natural Science Edition）
基金
陕西省自然科学基金
关键词
亚乙二硫基
二硫杂环戊烯
酮
衍生物
ethylenedithio 1, 3 dithiole 2 one
4,5 ethylenedithio 1.3 dithiole 2 thione
BEDT TTF intermediate synthesis
