摘要
本文介绍了一种虫酰肼在红栎和胶枞树叶中的残留量分析方法。分析过程主要包括柱层析净化和液相色谱分析。分析物采用二极管阵列式（ｄｉｏｄｅ－ａｒａｙ）紫外检测器进行检测，柱型为ＲＰ－８，流动相为乙腈、二氧六环、甲醇和水。方法平均回收率为８４～９０％，最低检出浓度为００１２～００２２ｍｇ／ｋｇ。
A method was developed to determine tebufenozide in some forest leaves.The procedure mainly included column cleanup and liquid chromatographic with a diode-array UV detector set at 236 nm ,using an RP-8 column with a mobile phase of acetonitrile-dioxane-methanol-water.Mean recoveries for analysis ranged 84～90%,with coefficient of variation was 7～9%.Limits of detection were 0.012～0.022mg/kg.
出处
《农药》
CAS
北大核心
1998年第2期27-29,共3页
Agrochemicals
关键词
虫酰肼
红栎
胶枞树叶
残留树叶
残留分析
tebufenozide,forest leaves,residual analysis ,high performance liquid chromatography.
