摘要
采用气相色谱-质谱联用法测定多氯联苯(PCBs),具有良好的灵敏度和选择性,在对食品用纸包装容器及材料样品的检测时,样品只须进行简单的溶剂萃取-浓缩,不须任何净化过程。本方法对目标化合物的检测限量为1μg/kg,平均回收率≥95%,相对标准偏差为4.25%～10.34%。
Determination ofpolychlorinated biphenyls （PCBs） by GC-MS method showed good sensitivity and selectivity. In determining paper-made food packaging containers and materials, samples can be analyzed directly only after solvent extraction and concentration without any cleanup procedure. The detection limits, average recoveries and RSD of the method were 1μg/kg for target compounds, ≥95% and 4.25- 10.34%, respectively.
出处
《现代食品科技》
EI
CAS
2009年第4期444-446,共3页
Modern Food Science and Technology
基金
质检总局"关键技术标准推进工程"专项"人体安全重要技术标准研制"课题
关键词
多氯联苯
食品用纸包装容器及材料
气相色谱-质谱联用法
polychlorinated biphenyls （PCBs）
paper-made food packaging containers and materials
gas chromatograph-mass spectrometry （GC-MS）
