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Preparation and Characterization of Mesoporous Al-MCM-41 Layers Deposited on FeCrAl Metallic Foils by an In-situ Hydrothermal Method 被引量:2

Preparation and Characterization of Mesoporous Al-MCM-41 Layers Deposited on FeCrAl Metallic Foils by an In-situ Hydrothermal Method
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摘要 A new class of activated mesoporous Al-MCM-41 layers was deposited on Fe-CrAl metallic foils in the presence of cationic surfactant cetyltrimethylammonium bromide under basic conditions by an in-situ hydrothermal method. The characterization techniques including X-ray diffraction, nitrogen adsorption and transmission electron microscopy, as well as field-emission scanning electron microscopy were performed to investigate the pore structure and surface morphology of the Al-MCM-41 layers. The Al-MCM-41 materials are of amorphous structure but exhibit large BET surface area (up to 757.0 m2/g) and pore volume (up to 0.72 cm3/g), as well as a mean pore diameter of 3 nm. The layers deposited on the FeCrAl foils are continuous despite with a few of holes on the surface. A new class of activated mesoporous Al-MCM-41 layers was deposited on Fe-CrAl metallic foils in the presence of cationic surfactant cetyltrimethylammonium bromide under basic conditions by an in-situ hydrothermal method. The characterization techniques including X-ray diffraction, nitrogen adsorption and transmission electron microscopy, as well as field-emission scanning electron microscopy were performed to investigate the pore structure and surface morphology of the Al-MCM-41 layers. The Al-MCM-41 materials are of amorphous structure but exhibit large BET surface area (up to 757.0 m2/g) and pore volume (up to 0.72 cm3/g), as well as a mean pore diameter of 3 nm. The layers deposited on the FeCrAl foils are continuous despite with a few of holes on the surface.
作者 韦奇
出处 《Journal of Wuhan University of Technology(Materials Science)》 SCIE EI CAS 2009年第1期1-4,共4页 武汉理工大学学报(材料科学英文版)
基金 Funded by the National Natural Science Foundation of China (No.50502002) Scientific Research Common Program of Beijing Municipal Commission of Education (No. KM200610005016) Youth Foundation of Beijing University of Technology (No.00190)
关键词 mesoporous Al-MCM-4l silica layers FeCrAl metallic foils HYDROTHERMALSYNTHESIS porosity deposition mesoporous Al-MCM-4l silica layers FeCrAl metallic foils hydrothermalsynthesis porosity deposition
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