期刊文献+

极性大、难挥发和热不稳定的多组份体系的简易分析方法──快原子轰击质谱与纸层析和薄层层析的联用 被引量:3

Combinations of FABMS with PC and TLC for Analysis of Polar, Involative and Thermally Labile Mixtures
下载PDF
导出
摘要 本文介绍两种简便的分析方法──快原子轰击质谱与纸层析、薄层层析的联用,并举例说明了这两种方法在极性大、难挥发、热不稳定的多组份体系的分析中的应用。结果表明,方法操作简便、快速、经济实用,可作为传统的色质联用(GC/MS和LC/MS)的补充。 The combinatios of FABMS with PC and TLC and their application in the analyses of polar, involative and thermally labile mixtures were introduced in this paper. As two examples, a mixture of six amino acids and the hydrolysates of a gypenoside were analyzed by PC-FABMS and TLC-FABMS respectively. The results indicate that the two combinations are simple, effective, practical and easy to be popularized, they can be regarded as a complement to the conventioal combinations of MS with GC and LC.
出处 《质谱学报》 EI CAS CSCD 1998年第1期18-22,共5页 Journal of Chinese Mass Spectrometry Society
关键词 快原子轰击质谱 纸层析 薄层层析 联用 fast atom bombardment mass spectrometry paper chromato graphy thin-layer chromatog raphy
  • 相关文献

参考文献3

  • 1姚钟平,J Planar Chromatogr,1994年,7卷,410页 被引量:1
  • 2姚钟平,Rapid Commun Mass Spectrom,1994年,8卷,481页 被引量:1
  • 3Chang T T,Anal Chem,1984年,56卷,209页 被引量:1

同被引文献94

  • 1张凤霞,高清华.几种假冒抗生素类药品鉴别[J].中国乡村医药,2004,11(12):46-46. 被引量:2
  • 2汪秀月,贺子华,陈琪.诺氟沙星胶囊快速鉴别法[J].安徽医药,1999,3(2):27-27. 被引量:1
  • 3徐大雄.国际药品防伪打假动态[J].中国品牌与防伪,2006(1):70-73. 被引量:1
  • 4钱丽华,吴越,栾洁,葛晓莹.喹诺酮类抗菌药的快速薄层色谱鉴别[J].中国现代应用药学,2006,23(5):401-402. 被引量:5
  • 5Luftmann H. A simple device for the extraction of TLC spots : direct coupling with an electrospray mass speetromeler. Anal Bioanal Chem ,2004,378:964. 被引量:1
  • 6Pasilis SP, Kertesz V, Van Berkel GJ, et al. Using HPTLC/DESI - MS for peptide identificationin 1D separations of tryptic protein digests. Anal Bioanal Chem ,2008 ,391: 317. 被引量:1
  • 7Mukhopadhyay R. The Hunt for Counterfeit Medicine. Anal Chem, 2007,79 (7) :2622. 被引量:1
  • 8JIANG En-zhu(姜恩铸).Primary Study on the Pyrolysis Database of Antibiotics(抗生素热裂解库的初步建立).Thesis(学位论文).Beijing(北京):Peking Union Medical College(中国协和医科大学),2008. 被引量:1
  • 9Manna L,Valvo L. Development and validation of a fast reversed - phase ion - pairing liquid chromatographic method for simultaneous determination of eight cephalosporin antibiotics in pharmaceutical formulations. Chromatographia ,2004,60 ( 11/12 ) :645. 被引量:1
  • 10Chong XM, Hu CQ. Compilation of an ESI - MS library of b - lactam antibiotics for rapid identification of drugs. Chromatographia ,2008, 68(9/10) :759. 被引量:1

引证文献3

二级引证文献13

相关作者

内容加载中请稍等...

相关机构

内容加载中请稍等...

相关主题

内容加载中请稍等...

浏览历史

内容加载中请稍等...
;
使用帮助 返回顶部