摘要
以自制的芳基芳酰肼类化合物为原料,以NaBrO3/H2SO4为氧化体系,在室温下,将芳基芳酰肼类化合物氧化脱氢为芳基芳酰基偶氮化合物。产品的结构经元素分析、IR、1HNMR确证,收率为85%—93%。
A series of acyldiazenes compounds from home made adipyl dihydrazide were synthesized using oxidation system of NaBrO3/H2SO4.The products were confirmed by elemental analysis,IR and 1HNMR.The yields were about from 85% to 93%.
出处
《光谱实验室》
CAS
CSCD
2008年第6期1192-1194,共3页
Chinese Journal of Spectroscopy Laboratory
