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Synthesis and characterization ofα-{ 3-[2-hydroxy-3-(N-methyl-N-hydroxy-ethylamino)propoxy]propyl}-ω-butylpolydimethylsiloxanes 被引量:1

Synthesis and characterization ofα-{ 3-[2-hydroxy-3-(N-methyl-N-hydroxy-ethylamino)propoxy]propyl}-ω-butylpolydimethylsiloxanes
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摘要 α-{ 3-[2-hydroxy-3-(N-methyl-N-hydroxyethylamino)propoxy]propyl }-α-butylpolydimethylsiloxanes III with various molecu- lar weights were prepared by epoxy addition of α-[3-(2,3-epoxy-propoxy)propyl]-α-butylpolydimethylsiloxanes Ⅱ and N- methylmonoethanolamine. At each step, the outcome compounds were characterized through FT-IR and NMR spectra, the results showed that each step was successfully carried out and objective products were achieved. α-{ 3-[2-hydroxy-3-(N-methyl-N-hydroxyethylamino)propoxy]propyl }-α-butylpolydimethylsiloxanes III with various molecu- lar weights were prepared by epoxy addition of α-[3-(2,3-epoxy-propoxy)propyl]-α-butylpolydimethylsiloxanes Ⅱ and N- methylmonoethanolamine. At each step, the outcome compounds were characterized through FT-IR and NMR spectra, the results showed that each step was successfully carried out and objective products were achieved.
出处 《Chinese Chemical Letters》 SCIE CAS CSCD 2008年第10期1196-1198,共3页 中国化学快报(英文版)
基金 the Natural Science Foundation of Shandong Province(No.Y2006B22).
关键词 Anionic ring-opening polymerization Hydrosilylation Epoxy addition α-{3-[2-Hydroxy-3-(N-methyl-N-hydroxyethylamino)pro-poxy]propyl }-to-butylpolydimethylsiloxanes Anionic ring-opening polymerization Hydrosilylation Epoxy addition α-{3-[2-Hydroxy-3-(N-methyl-N-hydroxyethylamino)pro-poxy]propyl }-to-butylpolydimethylsiloxanes
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