摘要
采用对苯二胺或２－氨基－５－硝基苯磺酸为原料合成了２，５－二氨基苯磺酸，后者收率可达到９５％，高于前者收率（小于６０％）．对铁屑还原反应的研究表明，铁屑粒度的降低以及采用本文制备的催化剂Ｂ，反应速率明显提高．
Diaminobenzenesulfonic acid has been synthesized from p phenylenediamine and 2-amino-5-nitrobenzenesulfonic acid. The product yield is about 95% from 2-amino-5-nitro-benzenesulfonic acid, which is more than from p phenylenediamine(which is less than 60%). The factors which can affect the reduction have been investigated. It is shown that by lowing the size of iron powder and by using the prepaired catalyte B the reaction rate becomes fast.
出处
《天津理工学院学报》
1997年第3期67-70,共4页
Journal of Tianjin Institute of Technology
