摘要
以叔丁硫醇为原料,经单质溴氧化得到了标题化合物,总收率92.3%。该方法反应时间短,收率较高,具有大规模生产价值。
Di-tert-butyldisumde was synthesized from tertbutylthiol as raw material by molecular bromine oxidation. The product yield reached 92.3 %, The method has high value for commercialization thanks to its convenient steps, simplicity and high product yield.
出处
《化学试剂》
CAS
CSCD
北大核心
2008年第9期709-710,共2页
Chemical Reagents
关键词
二叔丁基二硫醚
溴素
氧化
合成
di- tert-butyldisulfide
molecular bromide
oxidation
synthesis
