摘要
目的:建立冠心静胶囊的质量标准。方法:用薄层色谱法对川芎、冰片、赤芍、人参和三七进行定性鉴别;用高效液相色谱法对丹参中有效成分原儿茶醛进行定量测定。结果:定性鉴别斑点清晰,分离度好,易于区别;原儿茶醛平均加样回收率为99.91%,RSD=1.56%。结论:所建标准可用于冠心静胶囊的质量控制。
OBJECTIVE: To establish the quality standard of Guanxinjing capsule. METHODS.Ligusticum chuanxiong, Borneolum Syntheticum, Radix Paeoniae Rubra, Panax ginseng and Panax notogiseng were identified qualititively by TLC. The content of Protocatechuic aldehyde in salvia miltiorrhiza was determined by HPLC. RESULTS: The TLC spots were distinct and well-separated. The average recovery of the added sample was 99.91% and RSD was 1.56% . CONCLUSION: The established standard is suitable for the quality control of Guanxinjing capsule.
出处
《中国药房》
CAS
CSCD
北大核心
2008年第24期1894-1896,共3页
China Pharmacy