摘要
目的:建立十一味抗异散的质量标准。方法:采用薄层色谱法鉴别金银花、牡丹皮;高效液相色谱法测定盐酸小檗碱的含量。结果:薄层色谱斑点清晰,盐酸小檗碱在12～180μg·ml^(-1)之间呈良好的线性关系(r=0.9997),平均回收率为99.2%,RSD=0.5%(n=6)。结论:所建立的方法简便、准确、专属性强,可用于十一味抗异散的质量控制。
Objective： To establish the quality standard for Shiyiweikangyi Powders. Method： Flos Lonicerae, Cortex Moutan were identified by TLC,and the content of Berberine Hydrochloride was determined by HPLC. Result： The sports in TLC was fairly clear, Berberine Hydrochloride showed a good linear relationship in a ranger of 12 - 180 μg·ml^-1 （r = 0.999 7 ）. The average recovery was 99.2% with RSD 0.5% （ n = 6 ）. Conclusion： The methods is simple, accurate and specific, it can be used for the quality control of Shiyiweikangyi Powders.
出处
《中国药师》
CAS
2008年第6期637-639,共3页
China Pharmacist
关键词
十一味抗异散
金银花
牡丹皮
盐酸小檗碱
质量标准
Shiyiweikangyi Powders
Flos Lonicerae
Cortex Moutan
Berberine Hydrochloride
quality standard
