摘要
以相转移催化法合成了单体二烯丙基双酚Ｓ醚（ＤＡＢＳＥ），采用ＦＴＩＲ，１Ｈ－ＮＭＲ对单体结构进行了验证。ＤＳＣ结果表明：ＤＡＢＳＥ的熔点为１３３℃，热聚合温度高达２８０℃，并具有较宽的聚合峰。
Diallyl Bisphenol Sulfone Ether (DABSE) was synthesized by using the Phase Transfer Catalyst (PTC) method. The product was identified by FTIR and 1 H NMR spectra. The DSC results show that the compound melts at about 133℃ and that its thermal polymerization peak is wide with a maximum peak temperature at about 280℃.
出处
《北京化工大学学报（自然科学版）》
CAS
CSCD
1997年第3期22-25,共4页
Journal of Beijing University of Chemical Technology(Natural Science Edition)
关键词
二烯丙基
双酚S醚
DABSE
相转移催化
聚合
diallyl bisphenol salfone ether (DABSE)
phase transfer catalyst
FTIR
1H NMR
DSC
