摘要
建立火焰原子吸收光谱法测定地奥明七硫酸酯钠中钠含量的方法。采用标准曲线法,钠浓度在0.64-1.4mg·L^-1标准曲线范围内线性良好,相关系数为0.9991,加样回收率为100.3%,RSD为0.9%。结果6份样品测得钠的平均含量为0.1461mg·mg^-1,RSD为0.8%。实验结果表明,本法精密度高,准确性和重现性好,可用于控制地奥明七硫酸酯钠中钠的含量。
To establish a FAAS method to determine sodium in diosmin heptakis hydrogensulfate sodium. The good linearity was obtained when the concentration of sodium was within the range of 0.6-1.4mg·L^-1, the correlation coefficient is 0. 9991. The recovery ratio by standard addition is 100. 3%, and RSD is 0. 9%. The content of sodium in diosmin heptakis hydrogensulfate sodium is 0. 1461mg·mg^-1. The method is accurate with a good precision and reproduction.
出处
《中国药事》
CAS
2008年第3期233-234,共2页
Chinese Pharmaceutical Affairs
关键词
火焰原子吸收光谱法
钠
地奥明七硫酸酯钠
flame atomic absorption spectrophotometry
sodium
diosmin heptakis hydrogensulfate sodium