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水热法制备高老化比表面积铈锆复合氧化物及其性质表征 被引量:1

Synthesis of High-aging Specific Surface Area Ce-Zr Complex Oxide via Hydrothermal Method and Characterization
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摘要 以碳酸铈,碳酸锆作为原料,柠檬酸,硝酸作为添加剂,通过水热法制备出前驱物后,将其在600°C下煅烧得到铈锆复合氧化物Ce0.75Zr0.25O2和Ce0.4Zr0.6O2。将上述制备的复合氧化物经过980°C老化后即得到高老化比表面积铈锆复合氧化物,其比表面积为17.6 m2/g和19.0 m2/g。并对其性质进行了表征。 A precursor was made from cerium carbonate,zirconium carbonate,citric acid and nitric acid via hydrothermal method.Two Ce-Zr complex oxides,Ce0.75Zr0.25O2 and Ce0.4Zr0.6O2,were formed after calcination at 600(℃).Then the above oxides were aged at 980(℃),and two high-aging specific surface area Ce-Zr complex oxides were obtained with the specific surface area of 17.6 m^2/g and 19.0 m^2/g,respectively.Moreover,the properties of the products were characterized.
机构地区 同济大学化学系
出处 《化学世界》 CAS CSCD 北大核心 2008年第2期68-70,共3页 Chemical World
关键词 高老化比表面积 水热法 复合氧化物 high-aging specific surface area hydrothermal method complex oxide
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