摘要
目的:对复方金参胶囊中人参茎叶总皂苷的薄层鉴别以及含量测定进行研究。方法:利用薄层色谱法和高效液相色谱法技术,建立了复方金参胶囊中人参茎叶总皂苷的质量控制方法。结果:复方金参胶囊供试品色谱中,在与人参皂苷Re和人参皂苷Rg1对照品色谱相应的位置上,显相同颜色的斑点;人参皂苷Re在0.9216mg~9.2160mg(r=0.9999)范围内,峰面积与质量呈良好的线性关系;平均回收率为101.18%,RSD为1.39%(n=6)。结论:本文所建立的方法分离度好,简便易行,具有良好的重现性,可用于复方金参胶囊中人参茎叶总皂苷含量的测定。
Objective:To determine the content of total ginsenoside in fufang jinsheng capsule.Methods:TLC.HPLC methods were developed for the determination of total ginsenoside in fufang jinsheng capsule.Results'The samples and the reference substances have the same spots in TLC.The standard curves of ginsenoside-Re showed a good linearity and the average recoveries was 101.18% with RSD=1.39% (n=6).Conclusion:The method is quick, simple, and repeatable for the content determination of total gin-senoside in fufang jinsheng capsule.
出处
《中国药物应用与监测》
CAS
2008年第1期20-22,共3页
Chinese Journal of Drug Application and Monitoring
关键词
复方金参胶囊
人参茎叶总皂苷
含量测定
Fufang jinsheng capsule
Total ginsenoside in stem and leaf
Content determination