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火试金法测定精炼金的金含量 被引量:21

Determination of gold in refined gold by fire assaying method
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摘要 介绍了用火试金法测定精炼金(99.509/5~99.99%,w%)中金的含量。讨论了称样量,银、铅的加入量,灰吹温度,碾片厚度及长宽,分金温度,分金时间等因素的影响。对英国伦敦黄金白银市场协会(LBMA)的样品进行分析,相对标准偏差小于0.00319/6,极差小于0.0119/5,测定值与认证值相符。 The determination of gold content in refined gold (99. 50%-99. 99%,w%) in the fire assaying method was introduced. The effects of sample quantity, addition of silver and lead, cupellation temperature, thickness and length of grind piece, temperature and time for cupellation were investigated. Samples from London Bullion Market Association (LBMA) were analysed. RSD of the results was less than 0.003 1 %, and the range were less than 0. 011%. The results were in accordance with certified value.
出处 《冶金分析》 EI CAS CSCD 北大核心 2008年第1期71-73,共3页 Metallurgical Analysis
关键词 火试金法 精炼金 金含量 fire assaying method refined gold content of gold
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参考文献4

  • 1蔡树型,黄超.贵金属分析(Preciou smetal analysis)[M].北京:冶金工业出版社. 被引量:1
  • 2GB/15429.1-94合质金化学分析方法[s]. 被引量:1
  • 3GB/T11066.1-2-1989金化学分析方法[s]. 被引量:1
  • 4美国材料协会标准ASTMB562-595. 被引量:1

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