摘要
豆科植物含有一种荧光物质,对高效液相色谱/荧光检测(HPLC/FD)测定抗蚜威残留有干扰,易产生假阳性结果。通过薄层色谱(TLC)分离富集荧光物质,气相色谱/质谱(GC/MS)分析鉴定,该化合物为1,2-苯二甲酸,单(2-乙基己基)酯。建立GC/MS/SIM对豆科植物中抗蚜威残留检测方法。
A fluorescent composition in pea plant was interfered the determination of primicarb residue by high performance liquid chromatography/fluorescence diction （HPLC/FD）. The fluorescent composition was separated by thin layer chromatography （TLC）, identified by GC/MS, it was 1,2-benzendicarboxylic acid, mono （2-ethylhexyl） ester. An analytical method determined the primicarb residue in pea plant by GC/MS/SIM was developed.
出处
《农药》
CAS
北大核心
2008年第2期120-121,124,共3页
Agrochemicals
基金
云南省农业科技攻关资助项目(2006NG01)
