摘要
建立了一种测定1氨基4溴蒽醌2磺酸的高效液相色谱(HPLC)方法。以甲醇—水为流动相,四丁基溴化铵为离子对试剂,2萘酚为内标物,检测波长为240nm,线性范围为0~018mg/ml,浓度测定的变异系数为020%~034%。
The method was studied in RP HPLC analysis of 1 amino 4 bromo anthraquinone 2 sulfonic acid.Chromatographic conditions are with methanol water as mobile phase,tetrabutylammonium bromide as ion pair reagent,2 naphthol as internal standard and UV detection at 240nm.The method gave a linear range of 0~0.18mg/ml and a coefficient of variation of 0.20%~0 34%
出处
《精细化工》
EI
CAS
CSCD
北大核心
1997年第2期39-41,共3页
Fine Chemicals