摘要
采用FID检测器,使用DB-5毛细色谱柱,程序升温测定聚四氢呋喃工艺过程中的有机物含量。按照实验所确定的各种分析条件进行分析,使得各组分都得到了很好的分离,分离度均在1.5以上,回收率在98.4%~100.2%之间,分析结果比较准确可靠。
The Organics of the PTMEG producing process was chromatographed on DB -5 capillary column using temperature programmer and flame ionization detector. Under the determined conditionds, the component in the PTMEG production process were separated with good conduction and the known separated components were identified. The method was accurate and repeatable,The recoveries of this method were in the range of 98.4 % - 100.2 %.
出处
《辽宁化工》
CAS
2007年第11期787-789,共3页
Liaoning Chemical Industry
关键词
气相色谱法
毛细色谱柱
分离度
Gas Chromatography
Capillary column
Degree of separation