摘要
目的定性、定量分析桂枝挥发油成分。方法采用气相色谱-质谱检测,通过化学计量学解析法对二维色谱/质谱数据进行解析,得到各组分的纯色谱曲线和质谱,从而实现对桂枝挥发油成分的定性、定量分析。结果鉴定了33个桂枝挥发油成分,占挥发油成分总含量的81.32%。结论桂枝挥发油主要成分为Benzylidenemalonaldehyde(52.20%),Acetophenone(3.04%),3-(2-methoxyphenyl)-2-Propenal(2.20%),和1-(1,5-dimethyl-4-hexenyl)-4-methyl-Benzene(1.84%)。
Objective Qualitative and quantitative analysis for the volatile chemical components of Ramulus cinnamomi (RC). Methods Gas chromatography-mass spectrometry (GC-MS), chemometric resolution method (CRM) , and normalization methods were employed. Results Thirty-three volatile chemical components of RC were determined, accounting for 81.32% of total contents of volatile chemical components of RC. Conclusion The main volatile chemical components of RC are benzylidenemalonaldehyde,acetophenone,3-( 2-methoxyphenyl)-2-propenal and 1-( i,5-dimethyl-4-hexenyl) -4-methyl-benzene.
出处
《现代中药研究与实践》
CAS
2007年第3期31-34,共4页
Research and Practice on Chinese Medicines
基金
国家自然科学基金(No20235020)
关键词
桂枝
挥发油成分
GC/MS
化学计量学解析法
Ramulus Cinnamomi (RC), volatile chemical components, GC-MS, chemometric resolution method ( CRM)