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桂叶油热解产物的GC/MS分析 被引量:4

Analysis of Pyrolysis Products of Cinnamon Leaf Oil by Gas Chromatography/Mass Spectrometer
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摘要 采用GC/MS法分析了在250、300、400、500、600、700、800和900℃下桂叶油的热解产物,并用归一化法进行了定量。结果表明:①桂叶油在250℃以下不热解,丁香酚、β-石竹烯和乙酰丁香酚是桂叶油的主要致香成分;②600℃以下桂叶油主要释放出丁香酚和乙酰丁香酚等52种化合物;③700℃以上桂叶油不释放致香物质,而释放芳烃和稠环芳烃等有害物质,且其种类及相对含量均随着热解温度的升高而增大;④桂叶油的热解产物可能主要是丁香酚裂解形成的。 At 250, 300, 400, 500, 600,700, 800 and 900℃, the pyrolysis products of cinnamon leaf oil were analyzed by gas chromatography/mass spectrometry, and the relative content of the pyrolysis products were also calculated by normalization method. The results indicated that: 1 ) cinnamon leaf oil was not pyrolysised at 250℃ , and released out of flavor substances, such as eugenol,β- caryophyllene and aceteugenol; 2)under 600℃ ,52 pyrolysis products were released from the essence; 3)above 700℃ , no flavor was found in the pyrolysis products. Furthermore, with the raise of pyrolysis temperature, harmful substances were released, such as aromatic, polycyclic aromatic hydrocarbons; and the category and relative content of them increased with the temperature; 4)the pyrolysis products of cinnamon leaf oil were mainly possible came from eugenol.
出处 《烟草科技》 EI CAS 北大核心 2007年第7期36-41,共6页 Tobacco Science & Technology
关键词 桂叶油 热解 气相色谱/质谱 Cinnamon leaf oil Pyrolysis GC/MS
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参考文献7

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