摘要
目的建立舒康栓中愈创木酚的含量测定方法。方法以气相色谱法测定愈创木酚的含量。结果愈创木酚在0.0882～0.7935mg.mL-1内峰面积与浓度线性关系良好(r=0.9997),平均回收率为98.5%,相对标准偏差(RSD)为0.3%(n=6)。结论该法操作简便准确,重现性好,可作为该制剂的定量分析方法。
OBJECTIVE To establish a new method for determination of guaiacol in Shukang Suppository. METHODS The contents of guaiacol were determined by GC on a Agilent 6890N gas chromatograph. RESULTS The calibration curve showed good linearity over the range of 0. 0882-0. 7935mg· mL^-1 （ r =0. 9997）. The average recovery was 98. 5% and the relative standard deviation was 0. 3% （ n = 6）. CONCLUSION The method was simple,and accurate with a good reproducibility and can be used as quantitative analysis method for Shukang Suppository.
出处
《齐鲁药事》
2007年第5期287-288,共2页
qilu pharmaceutical affairs
