摘要
目的:为了进一步研究与发展均三嗪衍生物的制备方法.方法:在丙酮介质中,三聚氯氰先后与N-甲基苯胺、甲醇反应,合成了N-甲基苯氨基-4,6-二甲氧基-1,3,5三嗪.结果:标题化合物经红外光谱和质谱对它进行了表征,筛选出了最佳的工艺条件.结论:制备方法简单,反应条件温和,效果良好.
Aim To study and develop synthetic methods of 1,3,5 - triazine derivatives further. Method In the medium of acetone, N - methyl- phenylamino-4,6 -dlmethoxy- 1,3,5 -triazine has been prepared by the reaction of cyanuric chloride, N -methylaniline and methanoL Results The product has been characterized by IR and MS, Furthermore, the best reaction conditions have been determined. Conclusion This method is simple with mild reaction condition and good effect.
出处
《宜春学院学报》
2006年第6期19-21,共3页
Journal of Yichun University
基金
江西省自然科学基金资助项目(NO.0520083)
江西省教育厅科技计划项目(赣教技字06268)
宜春市社会发展重点科技计划项目(编号:JXYC2005KNA010)
