摘要
一种环境友好样品处理技术———固相萃取技术被用于环境激素类物质邻苯二甲酸丁基苄基酯(BBP)痕量检测研究中。利用GC-ECD进行检测,借助于均匀设计法合理安排试验,通过计算机回归技术对C18固相萃取柱的萃取条件进行设计和优化,建立了相关的数学模型,找出了各因素对峰面积的影响规律。成功地确定优化的BBP固相萃取条件为:正己烷与丙酮配比30∶1、洗脱体积2.0ml、洗脱速率4.0ml/min、上样速率8.0ml/min。
Solid phase extraction（SPE） technology , which is one of environmental - friendly technologies of sample pretreatment, was employed in the trace analysis of Butylbenzyl phthalate（BBP）. Depend on GC - ECD, Several SPE factors of the analyte was optimized by homogeneous design and the related mathematical model was obtained by computer regressive analysis technology. The results showed hexane： acetone, elution volume, elution flow rate, sampling flow rate are 30 ： 1,2.0ml, 4.0ml/min, 8. 0ml/min, respectively.
出处
《茂名学院学报》
2006年第6期6-9,共4页
Journal of Maoming College
基金
茂名学院重点课题基金资助(203251)
