摘要
以甲氨酰二氰基甲基化钾为原料，在室温条件下，采用固液相表面接触法与过量氯乙酰氯反应，合成了具有多个功能基的丁酰胺类化合物4-氯-2，2-二氰基-N-氯乙酰基丁酰胺-3-酮，产率为11．2％；m．P．147．8～148、1℃；其结构经IR、^1H NMR确认．
A new 4-chloro-2,2-dicyano-N-chloroacetyl butanamide-3-ketone with the functional groups ,yield of 11.2% and m. p . of 147.8-148. 1℃was designed and synthesized by the reaction of potassium carbamyl-dicyanomethanide through the surface contact method of solid-liquid phase under room temperature . The target compound＇s structure was characterized by IR and ^1H NMR.
出处
《甘肃联合大学学报（自然科学版）》
2006年第5期40-42,共3页
Journal of Gansu Lianhe University :Natural Sciences
基金
忻州师范学院基金资助课题(20040702)
