摘要
参考磷酸在345～356℃时有强腐蚀性的特点，采有硫磷混合酸消解矿样．能使样品消解完全。本方法经加标校核证明．检测结果重现性好，准确度高。
Accordlng to the strong corrosion of phosphoric acid between 345 and 356 centigrade, the author decomposed the sample with sulfur-phosphorus mixture acid. It showed that the sample could be dissolved completely in this process. This analysis method was verified well accuracy and repeatability by running standard addition and recovery experiments.
出处
《环境科学与技术》
CAS
CSCD
北大核心
2006年第B08期42-43,共2页
Environmental Science & Technology
关键词
EDTA滴定测定低冰镍
硫磷混合酸溶样
氟化钠除铁
过硫酸铵除锰
determination of low grade nickel matte by EDTA titration
decomposition with sulfur-phosphorus mixture acid
removal of Fe with NaF
removal of Mn with （NH4）2S2O8
