摘要
本文利用ＸＲＤ，ＳＥＭ，ＤＴＡ及ＢＥＴ等现代仪器，研究了Ｋ－Ｚｎ－Ｔｉ层状金属氧化物（ＬＭＯ）经ＨＡＣ，ＮＨ４Ｃｌ交换前后的基本性能。结果表明：该ＬＭＯ具有良好的离子交换性能，其面网间距由０．７８ｎｍ分别增加到０．８６ｎｍ和０．８８ｎｍ．同时，比表面积由２７ｍ２／ｇ分别增加到３０ｍ２／ｇ和５９ｍ２／ｇ，可望作为大孔分子筛的制备原料。
K-Zn-Ti layered metal oxide (LMO) is exchanged with acetic acid and ammonium chloride aqueous solution. XRD, SEM. DTA and BET techniques are used for. characterization of its basic property. It is shown that. K-Zn-Ti (LMO) possesses better ion-exchange property. After being exchanged with acetic acid and ammonium chloride. its interlayer distance (d value) increases to 0.86 nm and 0. 88 nm from 0. 78 nm, and its specific surface area increases to 30m2/g and 59m2/g from 27 m2/g respectively.
