摘要
利用同时蒸馏萃取法提取白玉兰精油中的挥发性成分,用气相色谱/质谱法鉴定出55种化学成分,占峰面积的97.73%,挥发油得率为3.81%。主要的化合物类别有烯类,烷类,醇类,醛类等。用面积归一化法测定了各种成分的相对质量分数,其中含量较高的组分有:w(桉叶油素)=16.52%,w〔4-甲基-1-异丙基-二环[3.1.0]己-2-烯〕=13.67%,w〔6,6-二甲基-2-亚甲基-二环[3.1.1]庚烷〕=12.78%,w(十五烷)=10.42%,w(β-月桂烯)=8.49%,w(D-柠檬烯)=4.42%,w(十氢-α,,α4 a-三甲基-8-亚甲基-2-萘甲醇)=4.08%,w〔(+)-α-松油醇〕=3.13%,w(大根香叶烯)=3.03%。
Volatile compounds of Magnolia denudate Desr. were collected using a simultaneous distillation and extraction （SDE） equipment. Fifty five constituents of the volatile were identified by GC/MS,which amounted to 97.73% of the total peak area. The compounds include olefins, alkanes, alcohols, aldehydes, etc. Relative contents of the constituents were determined by areanormalization method. The main constituents of the volatile were eucalyptol （ 16. 52 % ） ,4-methyl-1 - （1-methylethyl） - bicycle [ 3.1.0 ] hex-2-ene （ 13.67 % ）, 6,6-dimethy-2-methylene-bicyclo [ 3.1.1 ] heptane （ 12. 78 % ）, pentadecane （ 10. 42 % ） ,β-myrcene （ 8.49 % ）, D-limonene （ 4. 42 % ） , decahydro-α, α, 4 a-trimethyl-8- methylene-2-naphthalenemethanol （ 4. 08% ）, （ ＋ ）-α-terpineol （ 3. 13% ） and germacrene D （3.03%）.
出处
《精细化工》
EI
CAS
CSCD
北大核心
2006年第4期372-374,396,共4页
Fine Chemicals
关键词
白玉兰
同时蒸馏萃取
气相色谱/质谱
Magnolia denudate Desr.
simultaneous distillation and extraction
GC -MS
