摘要
用2,4-二硝基氟苯与各种取代的苯肼在DMSO中通过亲核取代反应合成了一系列氢化偶氮苯类化合物,其中8个是未见报道的新化合物,反应条件温和,反应时间短.后处理简便,收率93%~98%.
In this paper, a series of hydrazobenzenes were synthesized by the reaction of 2,4- dinitrofluorobenzene with substituted phenylhydrazines in DMSO. Among them, eight compounds have not reported. This method is mild, fast and easy work up. Moreover, the yields are excellent (93%-98%).
出处
《河南师范大学学报(自然科学版)》
CAS
CSCD
北大核心
2006年第1期87-90,共4页
Journal of Henan Normal University(Natural Science Edition)
关键词
2
4-二硝基氟苯
取代苯肼
亲核取代
2,4-dinitrofluorobenzene
substituted phenylhydrazines
substitution nucleophlilie