摘要
介绍了一种制备三羟甲基丙烷三丙烯酸酯（ＴＭＰＴＡ）的方法──酰氯法。用本法可得纯度＞９９．９％、收率＞９８％的题示产物。原理简单，途径简捷，无需阻聚剂，大大简化了后处理工艺，成本降低。
We recommend here a method of efficiently preparing high purity trimethylolpropane triacrylate. Using acrylic acid,thionyl chloride and trimethylolpropane as starting materials. We can make the product with percentage yield of >98% and a purity of>99.9%. The method we used is quit simple. Moreover due to the low reaction temperature,polymerization inhibitor is not needed. It will simplify the purification process,hence will reduce the cost.
出处
《精细化工》
CAS
CSCD
1996年第3期22-24,共3页
Fine Chemicals
基金
贵州科学院基金
