摘要
用高效液相色谱法同时测定生脉注射液中人参皂甙Rg1和Re含量。用十八烷基硅烷键合相柱,检测波长203nm,流动相为乙腈-0.05%磷酸溶液(18:82)。人参皂甙Rg1回收率为99.01%,RSD=1.58%:人参皂甙Re回收率为99.30%,RSD=1.30%。并对萃取方法进行了探讨。
In this paper we sueccssfully estabalished a HPLC method for the separation of Ginsenosides Rg1 and Re in sheng mai injection and quantitatively determinated Ginsenosides Rg1 and Re.The HLPC conditions were Inertsil ODS -2 column,CH3CN:0.05%H3PO4(18:82)as mobile phase,detection at 203 nm.The method was accurate,precise,sensitive and had a very Rood separatioin.
出处
《华西药学杂志》
CAS
CSCD
北大核心
1996年第1期19-22,共4页
West China Journal of Pharmaceutical Sciences