摘要
果蔬中２２种有机磷农残用ＣＧＣ－ＦＰＤ测定。采用带有电子压力控制（ＥＰＣ）的新型进样口系统，以电子压力编程（ＥＰＰ）方式控制载气流速，具有更高的检测灵敏度。用ＢＰ－１０毛细管柱为分离柱，２２种有机磷农药在４０ｍｉｎ内获得良好分离。本法对２２种有机磷农残的回收率范围为８２．５％～１０５．６％，变异系数为３．４％～１５．２％，检测限为０．１～２０×１０（－９）。
Determination of 22 organophosphorus pesticides residuein in fruits and vegetables was performed by CGC-FPD.Since we use the most new type of split/splitlees capillary injector system that equipped the EPC function, and control the carrier gas by EPP mode,so that a more high detection sensitivity has been got. The 22 organophosphorus pesticides residue could be good separation within 40 min on BP-10 capillary column.The RC and C.V.range for the method were 82.5%～105.6% and 3.4%～15.2% respectively,the detection limit range was 0.1～20×10-9
出处
《分析测试学报》
CAS
CSCD
1995年第3期68-71,共4页
Journal of Instrumental Analysis
关键词
毛细管色谱
有机磷农药
农药残留
蔬菜
Oganophosphorus pesticides residue,CGC-FPD,Determination.
