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PREPARATION OF MONODISPERSE CROSSLINKED POLYMER MICROSPHERES HAVING CHLOROMETHYL GROUP BY DISTILLATIONPRECIPITATION POLYMERIZATION 被引量：2

PREPARATION OF MONODISPERSE CROSSLINKED POLYMER MICROSPHERES HAVING CHLOROMETHYL GROUP BY DISTILLATIONPRECIPITATION POLYMERIZATION
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摘要 Monodisperse crosslinked poly(chloromethylstyrene-co-divinylbenzene)(poly(CMSt-co-DVB))microsphereswere prepared by distillation-precipitation copolymerization of chloromethylstyrene(CMSt)and divinylbenzene(DVB)inneat acetonitrile.The polymer particles had clean surfaces due to the absence of any added stabilizer.The size of the particlesranges from 2.59 μm to 3.19 μm and with mono-dispersity around 1.002-1.014.The effects of monomer feed incopolymerization on the microsphere formation were described.The polymer microspheres were characterized by SEM andchlorinity elemental analysis. Monodisperse crosslinked poly(chloromethylstyrene-co-divinylbenzene)(poly(CMSt-co-DVB))microsphereswere prepared by distillation-precipitation copolymerization of chloromethylstyrene(CMSt)and divinylbenzene(DVB)inneat acetonitrile.The polymer particles had clean surfaces due to the absence of any added stabilizer.The size of the particlesranges from 2.59 μm to 3.19 μm and with mono-dispersity around 1.002-1.014.The effects of monomer feed incopolymerization on the microsphere formation were described.The polymer microspheres were characterized by SEM andchlorinity elemental analysis.
作者 Shu-FengLi Xin-LinYang Wen-QiangHuang
机构地区 StateKeyLaboratoryofFunctionalPolymerMaterialsforAdsorptionandSeparation
出处 《Chinese Journal of Polymer Science》 SCIE CAS CSCD 2005年第2期197-202,共6页 高分子科学（英文版）
基金 This work was funded by the financial support of the National Natural Science Foundation of China(Project No.20274018) Nankai University.
关键词 Chloromethylstyrene DIVINYLBENZENE Distillation-precipitation polymerization CROSSLINKED MONODISPERSE Polymer microspheres Chlorinity. Chloromethylstyrene Divinylbenzene Distillation-precipitation polymerization Crosslinked Monodisperse Polymer microspheres Chlorinity.
分类号 TQ325 [化学工程—合成树脂塑料工业] TQ316.64
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同被引文献25

  • 1杨新林,黄文强.PREPARATION OF POLY(ETHYLENEGLYCOL-co-ACRYLIC ACID) MICROSPHERES WITH DIVINYLBENZNE AS CROSSLINKER BY DISTILLATION-PRECIPITATION POLYMERIZATION[J].Chinese Journal of Polymer Science,2007,25(3):303-309. 被引量：1
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  • 4Chen X, Zhou M, Hou Q, et al. Active Poly(4-chloromethyl styrene)-Functionalized Muhiwalled Carbon Nanotubes[J]. Macromolecular Chemistry and Physics, 2013, 214(16):1829-1835. 被引量：1
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  • 9Baruch-Sharon S, Margel S. Synthesis by a single-step swelling process and characterization of micrometer-sized polychloromethylstyrene/poly(butyl methacrylate) hemispherical composite particles of narrow size distribution[J]. Journal of Applied Polymer Science, 2008, 108(6):3727-3737. 被引量：1
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Chinese Journal of Polymer Science
2005年 第2期

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