摘要
报道了一个合成光导材料的单体N-乙烯咔唑的新方法,在KOH的二甲基亚砜溶液中,用常压乙炔将咔唑乙烯化,体系中水的含量以蒸馏法控制。N-乙烯咔唑的产率达到98%。本方法投资少,操作简便,产率高,可用于工业生产。
Abstract A new Mind of synthesis of N-vinylcar-bazole monomer was reported.The N-vinyla-tion of carbazole using acetyline was carriedout in the presence of KOH in DMSO at 145~150℃ under normal pressure. The water con-tent in the reaction svstem was controlled bydistillation,and N-vinylcarbazole was obtainedwith 98%yield.
出处
《精细化工》
CAS
CSCD
1994年第3期15-18,共4页
Fine Chemicals