摘要
本文研究了硫化氢与四氯化钛在某些有机介质中的反应，并提出了一个合成二硫化钛的新方法。该法是将干燥的硫化氢通入沸腾的四氯化铁的α－氯代萘溶液中，使硫化氢和四氯化钛发生复分解反应而生成二硫化钛。方法简便易行。Ｘ－射线物相鉴定及化学分析结果表明，产物为单一物相的、符合化学计量的二硫化钛。
This paper has studied the reactions of hydrogen sulphide with titanium tetrachloride in some organic mediums,and advanced a new method of synthesizing titanium disulphide.Titanium disulphide was synthesized by the double decomposition between dry hydrogen sulphide and titanium tetrachloride in boiling a-naphthalene chloride.The method is simple and convenient.The product is characterized by X-ray phase determination and chemical analysis.
出处
《化学工业与工程》
CAS
1994年第3期27-29,共3页
Chemical Industry and Engineering
关键词
二硫化钛合成
四氯化钛
硫化氢
s:titanium disulphide synthesis titanium tetrachloride hydrogen sulphide
