摘要
采用弱碱性无水碳酸钾作催化剂，结合真空精馏连续分离醋酸的工艺，由松油醇和醋酐合成了乙酸松油酯，摩尔得率达９２．４％，经真空蒸馏含量达９５．３％．该方法用于乙酸芳樟酯合成，产率也大于９０％．
Terpiyl acetate (Ⅰ) wits prepared in the yield of 92.4% by reaction of terpineol (Ⅱ)(α-, β-, and γ-Ⅱ were 84.7%, 7.40% and 3.0% respectively) with.Ac2O at 120 C in the presene of 4～5% of K2CO3 for 10 hours.
出处
《广西师院学报（自然科学版）》
1994年第1期48-50,共3页
Journal of Guangxi Teachers College(Natural Science Edition)
关键词
松油醇
乙酸松油酯
酯化
合成
香料
terpinyl acetate
terpineol
esterification
systhesis
