摘要
以固体Ti(SO4)2为催化剂,在微波条件下使α 萘乙酸和甲醇合成α 萘乙酸甲酯。最佳合成条件为:醇酸摩尔比为15∶1,催化剂用量为α 萘乙酸的10%,微波辐射时间为23min,微波功率为600W,产率为82.5%。
The methyl α-naphthylacetate was synthesized by α-naphthylacetic acid and methanol with (Ti(SO_4)_2) as catalyst under microwave irradiation. The optimum reaction conditions are as follows: the mole ratio of methanol to α-naphthylacetic is 15∶1,the catalyst is 10% of α-naphthylacetic acid,the reaction time is 23 min, the microwave power is 600 W. The yield is 82.5%.
出处
《应用化工》
CAS
CSCD
2004年第5期13-14,18,共3页
Applied Chemical Industry
基金
湖北省科技厅资助课题(2004AA1010C87)
关键词
Α-萘乙酸
甲醇
微波辐射
α-naphthylacetic acid
methanol
microwave irradiation
