摘要
目的:市售抗风湿药中怀疑含有激素物质,通过 TLC 法、HPLC 法鉴别药物中是否含有激素。方法:参照文献方法中泼尼松及其它甾体抗炎药的 TLC 方法以及醋酸泼尼松 HPLC 方法进行实验。结论:经 TLC 显色、HPLC 保留时间、以及 DAD 获得的 UV 图比较,确证抗风湿中药胶囊中含有醋酸泼尼。
Objective:The commercial antirheumatic traditional Chinese medicine is suspected that it contains hormaone matter,we decide to detect the capsules whether or not contains the hormone by TLC and HPLC Method We made the test according to the reference literature of the TLC method of prednisone or steroid antiinflammatory and the HPLC method of prednisone ac- etate.Conclusion:We validate the possibility that the capsules contains the prednisone acetate by contrast sample with standard material with the TLC coloured method、HPLC retained time method and the UV dagram from DAD.
出处
《黑龙江医药》
CAS
2004年第4期249-250,共2页
Heilongjiang Medicine journal
关键词
抗风湿药
中药
胶囊剂
醋酸泼尼松
定性鉴别
Antirheumatic
Traditional Chinese medicine
Prednisone acetate
Differentiation
