摘要
报道了α 羰基硫代甲酰胺与溴在三乙胺存在下的反应 ,合成了二 [( 1 芳基亚胺基 1 苯甲酰基 )甲基 ]二硫醚类化合物 ,产率为 60 %～ 65 %.它们的结构经元素分析、红外光谱。
Oxothioacetamide represents a class of stable and little explored compounds. The reaction of α oxothioacetamide with bromine in the presence of triethylamine was explored, and a new type of compounds called bis~[(1 arylimino 1 benzoyl)methyl] disulfide was obtained in 60%～65% yields and their structures were characterized by IR, NMR, MS spectra and elemental analyses.
出处
《有机化学》
SCIE
CAS
CSCD
北大核心
2004年第2期166-168,114,共4页
Chinese Journal of Organic Chemistry
基金
江苏省有机合成重点实验室 (No.T2 1 0 91 0 3)
苏州市科委 (No.SG 0 2 1 9)资助项目
