The crystal of [Ni（dien）2]2[Mn（NCS）6]·H2O was synthesized and the structure of its single crystal was determined by X ray diffraction. The crystal is monoclinic system, space group P21/c with a=16.544（3）,b=...The crystal of [Ni（dien）2]2[Mn（NCS）6]·H2O was synthesized and the structure of its single crystal was determined by X ray diffraction. The crystal is monoclinic system, space group P21/c with a=16.544（3）,b=15.137（2）, c=17.334（3）?, β=99.90（1）°, V=4276.3（12）?3, Z=4, Dc=1.479g·cm-3, Mr=951.55, F（000）=1998, μ=1.489mm-1, R=0.0399, Rw=0.0958. IR was also determined.展开更多
文摘The crystal of [Ni（dien）2]2[Mn（NCS）6]·H2O was synthesized and the structure of its single crystal was determined by X ray diffraction. The crystal is monoclinic system, space group P21/c with a=16.544（3）,b=15.137（2）, c=17.334（3）?, β=99.90（1）°, V=4276.3（12）?3, Z=4, Dc=1.479g·cm-3, Mr=951.55, F（000）=1998, μ=1.489mm-1, R=0.0399, Rw=0.0958. IR was also determined.
